FPC-TDC Spectrofluorometer

FPC-TDC Spectrofluorometer is a first photon counting system, ideal for detecting extremely low fluorescence signals. It is optimized for samples with low fluorescence yield, ensuring high sensitivity and time resolution.

Product SKU FPC-TDC Category Brand:

Description

⬛ FPC-TDC Spectrofluorometer

The FPC-TDC Spectrofluorometer is designed to study fluorescence decay in dim samples, where emitted light is extremely weak. Since fluorescence occurs on the nanosecond timescale (~10⁻⁸ s), the system uses a picosecond laser pulse to excite the sample and measures the time-of-flight of single photons emitted after deexcitation. Each detected photon passes through a monochromator and is captured by a photomultiplier, with the resulting photon arrival times reconstructing the full fluorescence decay profile.

To ensure accurate operation, the system maintains a low detection probability (<10% per pulse), making it exceptionally effective for samples with low fluorescence yield. The instrument is also adapted for electrochemical sample studies.

⬛ Quantities measured by the instrument include:

Fluorescence time decay as a function of wavelength and, in the case of electrochemical samples, polarization potential,
Emissive fluorescence spectrum,
I-V characteristics,
Open Circuit Potential (OCP),
Current flowing through the sample.

Spectrofluorometer modules

The system consists of:

  • Sample Chamber
  • Picosecond Laser
  • Monochromator for UV, VIS and IR range
  • Photomultiplier
  • Potentiostat
  • Electrochemical Cuvette with platinum electrode and reference Ag/AgCl electrode
  • Time to Digital Converter

Sample Chamber Interior

⬛ Optical path of laser beam and fluorescence light from the sample

Specification

Picosecond Laser

  • Wavelengths: 405 nm, 450-460 nm, 630-640 nm
  • Half width of the pulse duration: 150 ÷ 200 ps
  • Maximum pulse repetition frequency: 1 MHz
  • Light power of a pulse: 60 mW
  • Trigger type: TTL up to 1 MHz
  • Power supply: 12 VDC

⬛ Monochromator

  • Spectral range: 200 ÷ 1200 nm
  • Motorized slits, controlled via software
  • Entrance and output slit opening range: 0 ÷ 5 mm
  • Motorized internal shutter that provides full cut off of the light beam, controlled via software

⬛ Photomultiplier

R4998 Hammamatsu

  • Anode to Cathode voltage range: up to 2500 V
  • Spectral range: 300 ÷ 650 nm
  • Transit time spread (FWHM): 160 ps
  • Rise time: 0.7 ns

⬛ Time to Digital Converter

  • Time resolution: 27 ps
  • Maximum Measurement time: 500 ns
  • Additional Reference channel for laser jitter minimalization
  • Maximum impulse rate:
  • 500 kHz for 2 channels measurement: sample and reference
  • 1 MHz for 1 channel measurement
  • Internal trigger frequency: 1 kHz ÷ 1 MHz
  • External trigger mode, TTL input

⬛ Potentiostat

  • Bias potential range: -5 V ÷ 5 V
  • Current ranges: 10 nA, 100 nA, 1 µA, 10 µA, 100 µA, 1 mA, 10 mA
  • Current resolution: from 1 pA to 100 nA (range dependent)

⬛ Controller

  • Connection with PC: via USB 2.0
  • RS485 socket to control devices

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